A Short-Cut Design Technique to Batch Distillation Column — Oak Academic Publishing
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A Short-Cut Design Technique to Batch Distillation Column
Department of Applied Chemistry, School of Renewable Energy, Shenyang Institute of Engineering, Shenyang, China
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Liaoning Key Laboratory of Chemical Separation Technology, College of Chemical Engineering, Shenyang University of Chemical Technology, Shenyang, China
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Center for Natural Gas Hydrate Research, CAS Key Laboratory of Gas Hydrate, Guangzhou Institute of Energy Conversion, Chinese Academy of Sciences, Guangzhou, China
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Institute of Adsorption and Inorganic Membrane, State Key Laboratory of Fine Chemicals, Dalian University of Technology, Dalian, China
1 Department of Applied Chemistry, School of Renewable Energy, Shenyang Institute of Engineering, Shenyang, China
2 Liaoning Key Laboratory of Chemical Separation Technology, College of Chemical Engineering, Shenyang University of Chemical Technology, Shenyang, China
3 Center for Natural Gas Hydrate Research, CAS Key Laboratory of Gas Hydrate, Guangzhou Institute of Energy Conversion, Chinese Academy of Sciences, Guangzhou, China
4 Institute of Adsorption and Inorganic Membrane, State Key Laboratory of Fine Chemicals, Dalian University of Technology, Dalian, China
The effects of equipment parameters of batch distillation column on the yield proportion are discussed and analyzed, the relations between maximal yield proportion and the column equipment parameters are correlated, which not only can be used to appraise rationality of the design parameters of the columns being employed and which but also can be used to new batch distillation column design. Under the assistance of the separation difficulty defined in this paper, the minimum number of theoretical plates is determined by the limit loss proportion method given, and further the actual number of theoretical plates and the height for the batch distillation are calculated by using the redundancy coefficient found to complete the whole design of the batch distillation as shown in the computational sample. Research showed that the actual number of theoretical plates and the height of batch distillation column with the column diameter 0.6 m are 17 and 5.1 m in alcohol mixture separation system of the sample proposed. Moreover, the approach can be extended to the design of batch distillation column with a separation system of multi-component liquid mixture after those adjacent components are treated as numerous binary component systems.
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