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The High Surface Ratio Micro-MoS<sub>2</sub> Grain Composed of MoS<sub>2</sub> Nanosheet Prepared with One-Step Hydrothermal Synthesis
China-EU Institute for Clean and Renewable Energy, Huazhong University of Science and Technology, Wuhan, China
School of Optical and Electronic Information, Huazhong University of Science and Technology, Wuhan, China
School of Optical and Electronic Information, Huazhong University of Science and Technology, Wuhan, China
School of Optical and Electronic Information, Huazhong University of Science and Technology, Wuhan, China
China-EU Institute for Clean and Renewable Energy, Huazhong University of Science and Technology, Wuhan, China
School of Optical and Electronic Information, Huazhong University of Science and Technology, Wuhan, China
School of Optical and Electronic Information, Huazhong University of Science and Technology, Wuhan, China
China-EU Institute for Clean and Renewable Energy, Huazhong University of Science and Technology, Wuhan, China
School of Optical and Electronic Information, Huazhong University of Science and Technology, Wuhan, China
School of Optical and Electronic Information, Huazhong University of Science and Technology, Wuhan, China
School of Optical and Electronic Information, Huazhong University of Science and Technology, Wuhan, China
School of Optical and Electronic Information, Huazhong University of Science and Technology, Wuhan, China
School of Optical and Electronic Information, Huazhong University of Science and Technology, Wuhan, China
- 1 China-EU Institute for Clean and Renewable Energy, Huazhong University of Science and Technology, Wuhan, China
- 2 School of Optical and Electronic Information, Huazhong University of Science and Technology, Wuhan, China
- 3 School of Optical and Electronic Information, Huazhong University of Science and Technology, Wuhan, China
- 4 School of Optical and Electronic Information, Huazhong University of Science and Technology, Wuhan, China
- 5 China-EU Institute for Clean and Renewable Energy, Huazhong University of Science and Technology, Wuhan, China
- 6 School of Optical and Electronic Information, Huazhong University of Science and Technology, Wuhan, China
- 7 School of Optical and Electronic Information, Huazhong University of Science and Technology, Wuhan, China
- 8 China-EU Institute for Clean and Renewable Energy, Huazhong University of Science and Technology, Wuhan, China
- 9 School of Optical and Electronic Information, Huazhong University of Science and Technology, Wuhan, China
- 10 School of Optical and Electronic Information, Huazhong University of Science and Technology, Wuhan, China
- 11 School of Optical and Electronic Information, Huazhong University of Science and Technology, Wuhan, China
- 12 School of Optical and Electronic Information, Huazhong University of Science and Technology, Wuhan, China
- 13 School of Optical and Electronic Information, Huazhong University of Science and Technology, Wuhan, China
Journal of Minerals and Materials Characterization and Engineering·Volume 06 (2018)·Pages 373–381·Published 9 April 2018·DOI10.4236/jmmce.2018.63026
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Abstract
Micro molybdenum disulfide was prepared with one-step hydrothermal method; the influence of reactant concentration and temperature on the surface ratio of micro-MoS 2 grain was investigated. Raman spectroscopy (Raman), X-ray diffraction (XRD), and Scanning electron microscopy (SEM) were used to characterize the structure, composition and morphology of MoS 2 . The results show that micro-MoS 2 grains were synthesized with one-step hydrothermal synthesis, and the morphology of micro-MoS 2 grains is like flower and sphere. The SEM figures indicate that the surface ratio of micro-MoS 2 grains is different and also show that the surface ratio of micro-MoS 2 grains can be improved by regulating reactant concentration and temperature. This research showed a method to improve the surface ratio of micro-MoS 2 grains.
KeywordsMicro-MoS<sub>2</sub>GrainHydrothermalOne-Step ReactionNanosheet
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