Discharge Characteristic of Micro-Arc Oxidation on Aluminum Alloy under the Changing Electrolyte Temperature
- 1 CRRC Nanjing Puzhen Co., Ltd., Nanjing, China
- 2 CRRC Nanjing Puzhen Co., Ltd., Nanjing, China
- 3 School of Materials Science & Engineering, Southwest Jiaotong University, Chengdu, China
- 4 School of Materials Science & Engineering, Southwest Jiaotong University, Chengdu, China
Abstract
The electrolyte temperature has a great influence on the performance of the coating prepared by micro-arc oxidation (MAO). The behavior of MAO discharge in the changing electrolyte temperature has been investigated. Compared to constant electrolyte temperature in conventional MAO process, the process has different discharge characteristics under the changing electrolyte temperature. The amplitude of pulse voltage was detected to study the change of discharge characteristic under the constant-current control of MAO power supply. Three successive discharge stages were differentiated by the variable the pulse voltage versus process time. Since there were significant changes in the sound, the sound signals were acquired and the audio analysis was used to describe the changing of the MAO discharge at different stages. Optical emission spectroscopy (OES) was employed in situ to unveil how the micro-discharge changed with the temperature increasing. Scanning electron microscopy (SEM) was used to characterize the morphology of the coatings on 6N01 aluminum alloy prepared by normal process with the constant-temperature control of the MAO electrolyte and by the process under the changing electrolyte temperature. A mode of film growth and micro-discharge was given to describe the effects of the changing electrolyte temperature in the whole MAO process.
- Yang, Y.H., Feng, G., Gu, Y.H., et al. (2021) Analysis on Corrosion of Aluminum-Based Micro-Arc Oxidation Coating. Anti-Corrosion Methods and Materials, 68, 404-412. https://doi.org/10.1108/ACMM-09-2020-2377
- Ekin, S., Faiz, M., Yakup, Y., et al. (2022) Influence of Electrolyte Compositions and Electrical Parameters on Thermal Properties of Micro-Arc Oxidized AZ91 Alloy. Journal of Materials and Engineering and Performance, 31, 1667-1678. https://doi.org/10.1007/s11665-021-06292-0
- Rios, J.M., Quintero, D., Castano, J.G., et al. (2022) Effect of EDTA Addition on the Biotribological Properties of Coatings Obtained from PEO on the Ti6Al4V Alloy in a Phosphate-Based Solution. Surfaces and Interfaces, 30, Article ID: 101857. https://doi.org/10.1016/j.surfin.2022.101857
- Sobolev, A., Kossenko, A. and Borodianskiy, K. (2019) Study of the Effect of Current Pulse Frequency on Ti-6Al-4V Alloy Coating Formation by Micro Arc Oxidation. Materials, 23, Article No. 3983. https://doi.org/10.3390/ma12233983
- Tran, Q.-P., Sun, J.-K., Kuo, Y.-C., et al. (2017) Anomalous Layer-Thickening during Micro-Arc Oxidation of 6061Al Alloy. Journal of Alloys and Compounds, 697, 326-332. https://doi.org/10.1016/j.jallcom.2016.11.372
- Li, Z.Y., Cai, Z.B., Cui, Y., et al. (2019) Effect of Oxidation Time on the Impact Wear of Micro-Arc Oxidation Coating on Aluminum Alloy. Wear, 426, 285-295. https://doi.org/10.1016/j.wear.2019.01.084
- Al Bosta, M.M.S. and Ma, K. (2014) Influence of Electrolyte Temperature on Properties and Infrared Emissivity of MAO Ceramic Coating on 6061 Aluminum Alloy. Infrared Physics & Technology, 67, 63-72. https://doi.org/10.1016/j.infrared.2014.07.009
- Raj, V. and Mubarak Ali, M. (2009) Formation of Ceramic Alumina Nanocomposite Coatings on Aluminium for Enhanced Corrosion Resistance. Journal of Materials Processing Technology, 209, 5341-5352. https://doi.org/10.1016/j.jmatprotec.2009.04.004
- Wang, X.F., Zhu, Z.T., Li, Y.X. and Chen, H. (2018) Characterization of Micro-Arc Oxidation Coatings on 6N01 Aluminum Alloy under Different Electrolyte Temperature Control Modes. Journal of Materials Engineering and Performance, 27, 1890-1897. https://doi.org/10.1007/s11665-018-3313-y
- Albella, J.M., Montero, I. and Martinez-Duart, J.M. (1987) A Theory of Avalanche Breakdown during Anodic Oxidation. Electrochimica Acta, 32, 255-258. https://doi.org/10.1016/0013-4686(87)85032-6
- Wang, L., Chen, L., Yan, Z. and Fu, W. (2010) Optical Emission Spectroscopy Studies of Discharge Mechanism and Plasma Characteristics during Plasma Electrolytic Oxidation of Magnesium in Different Electrolytes. Surface and Coatings Technology, 205, 1651-1658. https://doi.org/10.1016/j.surfcoat.2010.10.022