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Li<SUB>4</SUB>Ti<SUB>5</SUB>O<SUB>12</SUB> Synthesis with High Specific Surface Area and Single Phase
Department of Mechanical Systems Engineering, Faculty of Engineering, Aich University of Technology, Gamagori, Japan
Department of Mechanical Systems Engineering, Faculty of Engineering, Aich University of Technology, Gamagori, Japan
- 1 Department of Mechanical Systems Engineering, Faculty of Engineering, Aich University of Technology, Gamagori, Japan
- 2 Department of Mechanical Systems Engineering, Faculty of Engineering, Aich University of Technology, Gamagori, Japan
Journal of Materials Science and Chemical Engineering·Volume 03 (2015)·Pages 68–73·Published 8 September 2015·DOI10.4236/msce.2015.39009
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Abstract
We have investigated a novel Li 4 Ti 5 O 12 synthesis with high specific surface area, high crystallization and single phase and its mechanism. The method was performed with a solid phase synthesis by using CH 3 COOLi· 2 H 2 O and anatase TiO 2 via Li 2 TiO 3 as an intermediate in pre-sintering at 500 ° C and sintering at 750 ° C. This result showed specific surface area of 12 m <sup>2</sup> /g and single phase- Li 4 Ti 5 O 12 by applying the high specific surface anatase TiO 2 as a precursor.
KeywordsLi<SUB>4</SUB>Ti<SUB>5</SUB>O<SUB>12</SUB>Solid Phase SynthesisSpecific Surface AreaSEMTEM
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