Design and Characterization of a Horizontal Double Impinging Jet Cell: Determination of Flow Modes at the Surface of a Flat Electrode
- 1 Laboratoire de Chimie Physique, Université Félix Houphouet-Boigny, Abidjan, C?te d’Ivoire
- 2 Laboratoire de Thermodynamique de Traitement et Sciences des Surfaces et Interfaces, Institut National Polytechnique Félix Houphouet-Boigny, Yamoussoukro, C?te d’ivoire
- 3 Laboratoire d’Electrochimie Physique et Analytique, Ecole Polytechnique Fédérale de Lausanne, Sion, Suisse
- 4 Laboratoire d’Electrochimie Physique et Analytique, Ecole Polytechnique Fédérale de Lausanne, Sion, Suisse
- 5 Laboratoire de Chimie Physique, Université Félix Houphouet-Boigny, Abidjan, C?te d’Ivoire
- 6 Laboratoire d’Electrochimie Physique et Analytique, Ecole Polytechnique Fédérale de Lausanne, Sion, Suisse
Abstract
An electrochemical cell consisting of a double horizontal Impinging Jet Cell (IJC) has been conceived and characterized. The purpose of this system is the simultaneous electrodeposition of a composite metal/particle coating on both surfaces of a metal sheet. The silica particles imprint in the nickel matrix has allowed to distinguish four different flow areas onto the electrode namely the stagnation area, the radial flow area characterized by a higher flow speed, the return flow area that involves gravity effect, and the drainage area with a constant draining speed. Based on the limiting current evolution as a function of the Reynolds number, three flow modes were extracted: the Laminar Low Flow (LLF), the Laminar High Flow (LHF) and the Disturbance. The IJC investigated ensures a laminar flow for a large range of flow rate from a nozzle-to-sample distance of 19 mm and creates an laminar flow ovoid plan merged with the sample for the high flows.
- Croussier, J., Eyraud, M., Croussier, J.-P. and Roman, J.-M. (1992) Influence of Substrate on the Electrode Position of Nickel-Molybdenum Alloys. Journal of Applied Electrochemistry, 22, 749-755. http://dx.doi.org/10.1007/BF01027505
- Yeh, S.H. and Wan, C.C. (1994) Codeposition of SiC Powders with Nickel in a Watts Bath. Journal of Applied Electrochemistry, 24, 993-1000. http://dx.doi.org/10.1007/BF00241190
- Losiewicz, B., Stepien, A., Gierlot, D. and Budniok, A. (1999) Composite Layers in Ni-P System Containing TiO2 and PTFE. Thin Solid Films, 349, 43-50. http://dx.doi.org/10.1016/S0040-6090(99)00175-3
- Li, J., Sun, Y., Sun, X. and Qiao, J. (2005) Mechanical and Corrosion-Resistance Performance of Electrodeposited Titania-Nickel Nanocomposite Coatings. Surface and Coatings Technology, 192, 331-335. http://dx.doi.org/10.1016/j.surfcoat.2004.04.082
- Özkan, S., Hapçi, G., Orhan, G. and Kazmanli, K. (2013) Electrodeposited Ni/SiC Nanocomposite Coatings and Evaluation of Wear and Corrosion Properties. Surface and Coatings Technology, 232, 734-741. http://dx.doi.org/10.1016/j.surfcoat.2013.06.089
- Fink, C.G. and Prince, J.D. (1928) Codeposition of Copper and Graphite. Transactions of the American Electrochemical Society, 54, 315, 1928.
- Ger, M.-D. (2004) Electrochemical Deposition of Nickel/SiC Composites in the Presence of Surfactants. Materials Chemistry and Physics, 87, 67-74. http://dx.doi.org/10.1016/j.matchemphys.2004.04.022
- Thiemig, D., Bund, A. and Talbot, J.B. (2007) Electrocodeposition of Nickel Nanocomposites Using an Impinging Jet Electrode. Journal of the Electrochemical Society, 154, D510-D515. http://dx.doi.org/10.1149/1.2767415
- Dablé, P.J.M.R., Chaïnet, E., Yao, B. and Gossan, A. (2009) Conceiving of an Electrochemical Cell for In Situ Hydrodynamic Approach. The Open Chemical Engineering Journal, 3, 1-7. http://dx.doi.org/10.2174/1874123100903010001
- Stappers, L. and Fransaer, J. (2005) The Effect of Turbulence on the Electrodeposition of Composite Coatings. Journal of the Electrochemical Society, 152, C392. http://dx.doi.org/10.1149/1.1914745
- Low, C.T.J., Wills, R.G.A. and Walsh, F.C. (2006) Electrodeposition of Composite Coatings Containing Nanoparticles in a Metal Deposit. Surface and Coatings Technology, 201, 371-383. http://dx.doi.org/10.1016/j.surfcoat.2005.11.123
- Vaezi, M.R., Sadrnezhaad, S.K. and Nikzad, L. (2008) Electrodeposition of Ni-SiC Nano-Composite Coatings and Evaluation of Wear and Corrosion Resistance and Electroplating Characteristics. Colloids and Surfaces A: Physicochemical and Engineering Aspects, 315, 178. http://dx.doi.org/10.1016/j.colsurfa.2007.07.027