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Soft-Chemical Synthesis of Vanadium Oxide Nanostructures Using 3, 3’, 3”-Nitrilotripropionic Acid ( NTP) as a Carrier
Institut für Chemie, AG Elektrochemie, Technische Universit?t Chemnitz, D-09107 Chemnitz, Germany
- 1 Institut für Chemie, AG Elektrochemie, Technische Universit?t Chemnitz, D-09107 Chemnitz, Germany
- 2
- 3
Soft Nanoscience Letters·Volume 01 (2011)·Pages 66–70·Published 20 July 2011·DOI10.4236/snl.2011.13012
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Abstract
Vanadium oxide nanostructures were synthesized using NTP as a carrier through soft-chemical method. The influence of calcination temperature on the phase and morphology of obtained pristine product were characterized using X-ray diffraction (XRD), thermal gravimetric analysis (TGA) and scanning electron microscopy (SEM). Cyclic voltammogram studies were conducted to examine the electrochemical performance of cathodes made of vanadium oxide nanostructures. X-ray diffraction results show that, the particle size of the nanomaterials is increases with the increasing of calcination temperature.
KeywordsNanomaterialsSoft-Chemical MethodMorphologyCyclic Voltammogram
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